Predict the structure of the following compounds:
Formula: C4H8O (All scale is in ppm) (NMR Solvent: CDCl3)
Calculate the element of unsaturation of the compound.
1H NMR
Homework Answers
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Predict the structure of the following compounds:
Formula: C4H8O (All scale is in ppm) (NMR
Solvent:...
The 1H NMR spectrum has peaks (marked with "x") for a minor byproduct - what might...
The 1H NMR spectrum has peaks (marked with "x") for a minor
byproduct - what might that be?
7.4741 7.3572 7.3393 -5.4109 4.2023 4.1906 -4.1725 4.1608 -3.5350 -3.5065 -3.4775 Spectrometer: 400 MHZ Solvent: CDCI T 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 <3.2368 CDCI, x = peak from minor byproduct do 1.00-1 F-602 3.1444 Feer to 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 ppm 1.0 CHEM 08LB: 1H NMR...
Identify the peak in the 1H NMR spectrum corresponding to the CH3 group, explain what coupling...
Identify the peak in the 1H NMR spectrum corresponding to the
CH3 group, explain what coupling pattern it has and why it has that
pattern.
7.4741 7.3572 7.3393 -5.4109 4.2023 4.1906 -4.1725 4.1608 -3.5350 -3.5065 -3.4775 Spectrometer: 400 MHZ Solvent: CDCI T 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 <3.2368 CDCI, x = peak from minor byproduct do 1.00-1 F-602 3.1444 Feer to 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0...
identify the peak in the 1H NMR spectrum corresponding to the CH3 group, explain what coupling...
identify the peak in the 1H NMR spectrum corresponding to the
CH3 group, explain what coupling pattern it has and why it has that
pattern.
7.4741 7.3572 7.3393 -5.4109 4.2023 4.1906 -4.1725 4.1608 -3.5350 -3.5065 -3.4775 Spectrometer: 400 MHZ Solvent: CDCI T 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 <3.2368 CDCI, x = peak from minor byproduct do 1.00-1 F-602 3.1444 Feer to 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0...
Label peaks and determine the structure of the aldehyde in the 1H NMR and 13C1H NMR:...
Label peaks and determine the structure of the
aldehyde in the 1H NMR and 13C1H NMR:
pg 1H NMR of product from aldehyde Yin CDCI3 CHCI ppm Hz Intensity 17.73 3091.6 621.6 2 7.69 3075.7 690.3 3 7.59 3036.2 1108.5 4 7.57 3027.5 1199.0 5 6.98 2793.9 961.0 6 6.95 2779.9 1320.9 76.94 2778.0 1279.1 8 6.93 2771.1 1185.2 7.60 7.55 7.50 7.45 7.40 7.35 7.30 7.25 fl (ppm) 7.20 7.15 7.10 7.057.00 6.95 6.90 OK to group CHCl3 -...
Please answer the NMR tables for wintergreen and Pear, can you please make it as neat...
Please answer the NMR tables for
wintergreen and Pear, can you please make it as neat as possible
thanks!
WINTERGREEN
Pear
The procedure below is written as if you were conducting this experiment in the lab. You will nee to read through it carefully to complete the lab report and answer the questions appropriately For NMR analyses, complete the spectral assignments as shown in the example below. Example of a 'H-NMR analysis table: HoHo Ha Iodomethane Há На Chemical Shift...
A compound A, C7H12O3, contains two functional groups. One of the functional groups is a derivative...
A compound A, C7H12O3, contains two functional groups. One of the functional groups is a derivative of carboxylic acid. The 1H NMR spectrum of the compound is given below. Deduce the structure of the compound A. Write your structure on the spectrum and using arrows assign all the peaks in the spectrum to various protons in the molecule. (5 Pts, NO PARTIAL CREDITS) 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 3.2 3.1 3.0 2.9 2.8 2.7...
Match the peaks labeled A,B,C,D,E to the Diels-Adler product and what part of the products structure...
Match the peaks labeled A,B,C,D,E to the Diels-Adler
product and what part of the products structure creates each peak
on the NMR graph.
3.60 3.58 3.56 3.54 3.52 f1 (ppm) 3.50 3.48 3.46 C (dd) 7.34 7.45 7.40 7.35 7.30 7.25 i (ppm) 7,20 7.15 7.10 B (dd) A (dt) 7.39 7.20 D (t) 4.83 E (dd) 3.53 T T 1.98 1.93 4.00 2.09 2.01 .8 7.6 7.4 7.2 7.0 6.8 6.6 6.4 6.2 6.0 5.8 5.6 5.4 f1 (ppm)...
fill out the table below using the H-NMR there may be more or less noteable peaks....
fill out the table below using the H-NMR
there may be more or less noteable peaks.
the two most important are Bis-allylic protons and OCH3
Methoxylic protons
Below depicts the H-NMR products: Characterization of the Chemical shift of the peak (location) Integration value peak 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 3.2 3.1 3.0 2.9 2.8 Proton oza 20.90 619 : parts per Million : Proton
(a) From the spectral data ( H, C NMR, IR, MS) you were given, identify the...
(a) From the spectral data ( H, C NMR, IR, MS) you were given,
identify the structure of your product. Explain why you chose your
particular product based on the spectroscopic data.
(b) Fully assign the 1H NMR spectrum of your product (i.e.
determine which peaks in the 1H NMR correspond to which hydrogens
in the product). You will not receive full marks for determination
of the unknown unless you assign the 1H NMR spectrum
completely.
(c) Now work backwards...
Parametirc test or not: Test statistic: p-value: decision: Is There A Difference Between the Means?
Parametirc test or not:Test statistic:p-value:decision:Is There A Difference Between the Means?6.7 6.2 3.1 310.3 10 5 5.56.9 5.5 3.3 3.110.5 6.3 4.3 5.44.5 4.6 1.8 25.6 5.6 2 2.65.9 6.1 2.1 2.58 11.7 4 4.68 7.4 3.3 3.15.8 5.2 3.1 2.96 7.3 3.0 3.28.7 5.3 2.7 36 5.5 2.1 2.27.2 6.3 3.5 3.25.9 4.6 2.9 3.46 7.4 3 3.37.2 7.8 3.7 3.48.6 9.4 5.1 5.77.2 8.1 2.8 3.15.8 5.4 2.2 1.83.3 4 1.7 1.86.8 5.1 2 1.83.7 3.5 2.2 2.112...
The 1H NMR spectrum has peaks (marked with "x") for a minor
byproduct - what might that be?
7.4741 7.3572 7.3393 -5.4109 4.2023 4.1906 -4.1725 4.1608 -3.5350 -3.5065 -3.4775 Spectrometer: 400 MHZ Solvent: CDCI T 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 <3.2368 CDCI, x = peak from minor byproduct do 1.00-1 F-602 3.1444 Feer to 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 ppm 1.0 CHEM 08LB: 1H NMR...
Identify the peak in the 1H NMR spectrum corresponding to the
CH3 group, explain what coupling pattern it has and why it has that
pattern.
7.4741 7.3572 7.3393 -5.4109 4.2023 4.1906 -4.1725 4.1608 -3.5350 -3.5065 -3.4775 Spectrometer: 400 MHZ Solvent: CDCI T 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 <3.2368 CDCI, x = peak from minor byproduct do 1.00-1 F-602 3.1444 Feer to 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0...
identify the peak in the 1H NMR spectrum corresponding to the
CH3 group, explain what coupling pattern it has and why it has that
pattern.
7.4741 7.3572 7.3393 -5.4109 4.2023 4.1906 -4.1725 4.1608 -3.5350 -3.5065 -3.4775 Spectrometer: 400 MHZ Solvent: CDCI T 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 <3.2368 CDCI, x = peak from minor byproduct do 1.00-1 F-602 3.1444 Feer to 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0...
Label peaks and determine the structure of the
aldehyde in the 1H NMR and 13C1H NMR:
pg 1H NMR of product from aldehyde Yin CDCI3 CHCI ppm Hz Intensity 17.73 3091.6 621.6 2 7.69 3075.7 690.3 3 7.59 3036.2 1108.5 4 7.57 3027.5 1199.0 5 6.98 2793.9 961.0 6 6.95 2779.9 1320.9 76.94 2778.0 1279.1 8 6.93 2771.1 1185.2 7.60 7.55 7.50 7.45 7.40 7.35 7.30 7.25 fl (ppm) 7.20 7.15 7.10 7.057.00 6.95 6.90 OK to group CHCl3 -...
Please answer the NMR tables for
wintergreen and Pear, can you please make it as neat as possible
thanks!
WINTERGREEN
Pear
The procedure below is written as if you were conducting this experiment in the lab. You will nee to read through it carefully to complete the lab report and answer the questions appropriately For NMR analyses, complete the spectral assignments as shown in the example below. Example of a 'H-NMR analysis table: HoHo Ha Iodomethane Há На Chemical Shift...
A compound A, C7H12O3, contains two functional groups. One of the functional groups is a derivative of carboxylic acid. The 1H NMR spectrum of the compound is given below. Deduce the structure of the compound A. Write your structure on the spectrum and using arrows assign all the peaks in the spectrum to various protons in the molecule. (5 Pts, NO PARTIAL CREDITS) 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 3.2 3.1 3.0 2.9 2.8 2.7...
Match the peaks labeled A,B,C,D,E to the Diels-Adler
product and what part of the products structure creates each peak
on the NMR graph.
3.60 3.58 3.56 3.54 3.52 f1 (ppm) 3.50 3.48 3.46 C (dd) 7.34 7.45 7.40 7.35 7.30 7.25 i (ppm) 7,20 7.15 7.10 B (dd) A (dt) 7.39 7.20 D (t) 4.83 E (dd) 3.53 T T 1.98 1.93 4.00 2.09 2.01 .8 7.6 7.4 7.2 7.0 6.8 6.6 6.4 6.2 6.0 5.8 5.6 5.4 f1 (ppm)...
fill out the table below using the H-NMR
there may be more or less noteable peaks.
the two most important are Bis-allylic protons and OCH3
Methoxylic protons
Below depicts the H-NMR products: Characterization of the Chemical shift of the peak (location) Integration value peak 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 3.2 3.1 3.0 2.9 2.8 Proton oza 20.90 619 : parts per Million : Proton
(a) From the spectral data ( H, C NMR, IR, MS) you were given,
identify the structure of your product. Explain why you chose your
particular product based on the spectroscopic data.
(b) Fully assign the 1H NMR spectrum of your product (i.e.
determine which peaks in the 1H NMR correspond to which hydrogens
in the product). You will not receive full marks for determination
of the unknown unless you assign the 1H NMR spectrum
completely.
(c) Now work backwards...
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