Question

Please read the statement below and kindly produce by drawing with aid of chemical drawing software;

A synthetic pathway for the stated reaction, showing all the curly arrows from beginning to end (Mechanism)
In detail, 6.0 g ß-CD, beta-Cyclodextrin (previously dried at 100.0°C for 12 h) was dissolved in a mixture of 40.0 mL of dried N,N-dimethylformamide (DMF) and 14.0 mL of dried triethylamine (TEA) while magnetically stirred for more than 20 min. Then, 5.0 mL of acryloyl chloride was slowly dropped into the mixture at 0°C while in an atmosphere of nitrogen. The resulting mixture was stirred for another 30 min at room temperature and then vacuum-filtrated. Then, acetone was added to the filtrate drop by drop to obtain a precipitation product. The solvent was removed, and the precipitate was washed with acetone at least three times to further purify the product. Finally, the precipitate was collected and dried at room temperature under a vacuum.

Thank you

beta CD means; beta-Cyclodextrin

Answer 1