For a scientific report, write a detailed method for synthesising aspirin in a lab by using...
For a scientific report, write a detailed method for synthesising aspirin in a lab by using salicylic acid and acetic acid as the reactants (acetic anhydride is unavailable).
Homework Answers
It is possible to produce aspirin using salicylic acid and acetic acid . Take acetic acid and salicylic acid and sodium acetate . Heat it for a while ( say one and half hour ) and then pour the reaction mixture in ice-water to get solid aspirin. The phenol group in salicylic acid froms an ester with carboxylic part of acetic acid . The excess water and presence of an acid catalyst , the reaction will proceed in reverse direction . That is hydrolysis of ester . This makes this reaction slow and low yielding.
If you use acid anhydride that reaction is fast and higher yielding because acid anhydride is more reactive than carboxylic acid.
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For a scientific report, write a detailed method for
synthesising aspirin in a lab by using...
Aspirin can be synthesized in the lab by combining salicylic acid (C7H6O3) and acetic anhydride (C4H6O3)...
Aspirin can be synthesized in the lab by combining salicylic acid (C7H6O3) and acetic anhydride (C4H6O3) to form aspirin (C9H8O4) and acetic acid (C2H4O2).C2H4O2). The balanced equation for this reaction is C7H6O3+C4H6O3⟶C9H8O4+C2H4O2 A student started with 4.00 mL acetic anhydride (density=1.08 g/mL) and 2.07 g salicylic acid. The student synthesized 2.00 g of aspirin. Select the limiting reactant. acetic acid (C2H4O2) salicylic acid (C7H6O3) aspirin (C9H8O4) acetic anhydride (C4H6O3) Calculate the theoretical yield of aspirin (C9H8O4). theoretical yield: Calculate the...
Organic chemistry -Carboxylic acid homework Question: In the general chemistry lab, students synthesize aspirin from salicylic...
Organic chemistry -Carboxylic acid homework
Question: In the general chemistry lab, students synthesize
aspirin from salicylic acid and acetic anhydride. In the lab,
students use sulfuric acid as a catalyst, but I want to consider an
alternate method for synthesizing aspirin using sodium acetate as a
catalyst:
a. Draw the structure of sodium acetate. Is sodium acetate a
stronger or weaker base than sodium hydroxide (NaOH). Explain. (1.5
pts)
b. Consider the structure of salicylic acid. It contains two
potentially...
Aspirin can be sunthesized in the lab by combining salicylic acid (C7H6O3) and acetic anhydride (C4H6O3)...
Aspirin can be sunthesized in the lab by combining salicylic acid (C7H6O3) and acetic anhydride (C4H6O3) to form aspirin (C9H8O4) and acetic acid (C2H4O2). The balanced equation for this reaction is C7H6O3+C4H6O3⟶C9H8O4+C2H4O2 A student started with 4.45 mL acetic anhydride (density=1.08 g/mL) and 2.34 g salicylic acid. The student synthesized 2.47 g of aspirin. Calculate the theoretical yield of aspirin (C9H8O4) in grams Calculate the percent yield for aspirin (C9H8O4)
Exercise 7: The % Yield of Aspirin Name Date Read Exercise 7 in your lab manual....
Exercise 7: The % Yield of Aspirin Name Date Read Exercise 7 in your lab manual. Complete the Pre-lab Assignment. In this substitute lab exercise, you will watch a short video on preparing aspirin. The video is posted on the course Moodle page, and it provides the masses of the reactants and the product; you should be able to calculate the theoretical yield and the % yield from the data given by the video. Submit the completed assignment by March...
- OF ASPIRIN ANU UN riment Exercise 7: The Yield of Aspirin Name Date Pred the...
- OF ASPIRIN ANU UN riment Exercise 7: The Yield of Aspirin Name Date Pred the el the st Read Exercise 7 in your lab manual. Complete the Pre-lab Assignment In this substitute lab exercise, you will watch a short video on preparing aspirin. The videos posted on the course Moodle page, and it provides the masses of the reactants and the product; you should be able to calculate the theoretical yield and the yield from the data given by...
Lab Section Nume Preparation and Examination of a Drug: Aspirin EXPERIMENT 25 OBSERVATIONS AND RESULTS 1....
Lab Section Nume Preparation and Examination of a Drug: Aspirin EXPERIMENT 25 OBSERVATIONS AND RESULTS 1. The Synthesis of Aspirin Record the weight of your aspirin, and calculate the percentage yield. Base the yield on salicylic acid since we acetic anhydride was used. Show all calculations. Weight of aspirin d. 08035 Yield of aspirin 2. Contaminants in Aspirin What was the color of the salicylic acid-ferric chloride test solution? On the basis of color is either your aspirin or commercial...
1. [05 pts.] Draw the chemical equation for preparation of Aspirin. (No mechanism) 2. [15 pts.)...
1. [05 pts.] Draw the chemical equation for preparation of Aspirin. (No mechanism) 2. [15 pts.) Show the detailed mechanism movement of electrons. for reaction. Show all arrow to indicate 3. [09 pts.] Briefly explain the roles of Salicylic acid, Acetic anhydride and phosphoric acid in the reaction. 4. [05 pts.] What type of reaction is preparation of Aspirin? 5. [06 pts.] Briefly describe esterification and give an example using Acyl chloride as one of the reactants.
Show the calculation of (1) the expected grams of aspirin (CgHg04) formed in the reaction of...
Show the calculation of (1) the expected grams of aspirin (CgHg04) formed in the reaction of 2.5 grams of salicylic acid (C7H6O3) with excess acetic anhydride and then show the calculation of (2) the % yield if the actual yield of aspirin is 1.89 grams. Reaction is shown below: O. OH соон ООН Acetic Anhydride Salicylic acid ASPRIN Acetylsaicyic acid BACKNE REPORT A PROBLEM All Rights Reserved Design
can you please help me with this !!! which ever you can is fine, please... thanks...
can you please help me with this !!!
which ever you can is fine, please... thanks !
Results/Data • Aspirin synthesis salicylic acid: 2.0 g Acetic anhydride: 2 mL d= 1.082g/ml sodium acetate: 0.4 g • Experimental yield of aspirin: 2.4 g REPORT DATE: NAME: LAB PARTNER: I PREPARATION OF METHYL SALICYLATE (OIL OF WINTERGREEN): Reaction Odor: Color after addition of FeCl solution: Control Odor: Color after addition of FeCl3 solution: Question Which functional group of salicylic acid forms a...
please help me ! do you think this is good so far ? Results/Data • Aspirin...
please help me ! do you think this is good so far ?
Results/Data • Aspirin synthesis salicylic acid: 2.0 g Acetic anhydride: 2 mL d= 1.082g/mL sodium acetate: 0.4 g • Experimental yield of aspirin: 2.4 g FORMATION OF ESTERS II. PREPARATION OF ACETYL SALICYLIC ACID (ASPIRIN): 1 Complete the table below by entering appropriate values into the empty boxes. Show calculations for all entries clearly below. Reactants Chemical MW Grams of Moles of Moles of Limiting Melting Formula...
Organic chemistry -Carboxylic acid homework
Question: In the general chemistry lab, students synthesize
aspirin from salicylic acid and acetic anhydride. In the lab,
students use sulfuric acid as a catalyst, but I want to consider an
alternate method for synthesizing aspirin using sodium acetate as a
catalyst:
a. Draw the structure of sodium acetate. Is sodium acetate a
stronger or weaker base than sodium hydroxide (NaOH). Explain. (1.5
pts)
b. Consider the structure of salicylic acid. It contains two
potentially...
Exercise 7: The % Yield of Aspirin Name Date Read Exercise 7 in your lab manual. Complete the Pre-lab Assignment. In this substitute lab exercise, you will watch a short video on preparing aspirin. The video is posted on the course Moodle page, and it provides the masses of the reactants and the product; you should be able to calculate the theoretical yield and the % yield from the data given by the video. Submit the completed assignment by March...
- OF ASPIRIN ANU UN riment Exercise 7: The Yield of Aspirin Name Date Pred the el the st Read Exercise 7 in your lab manual. Complete the Pre-lab Assignment In this substitute lab exercise, you will watch a short video on preparing aspirin. The videos posted on the course Moodle page, and it provides the masses of the reactants and the product; you should be able to calculate the theoretical yield and the yield from the data given by...
Lab Section Nume Preparation and Examination of a Drug: Aspirin EXPERIMENT 25 OBSERVATIONS AND RESULTS 1. The Synthesis of Aspirin Record the weight of your aspirin, and calculate the percentage yield. Base the yield on salicylic acid since we acetic anhydride was used. Show all calculations. Weight of aspirin d. 08035 Yield of aspirin 2. Contaminants in Aspirin What was the color of the salicylic acid-ferric chloride test solution? On the basis of color is either your aspirin or commercial...
1. [05 pts.] Draw the chemical equation for preparation of Aspirin. (No mechanism) 2. [15 pts.) Show the detailed mechanism movement of electrons. for reaction. Show all arrow to indicate 3. [09 pts.] Briefly explain the roles of Salicylic acid, Acetic anhydride and phosphoric acid in the reaction. 4. [05 pts.] What type of reaction is preparation of Aspirin? 5. [06 pts.] Briefly describe esterification and give an example using Acyl chloride as one of the reactants.
Show the calculation of (1) the expected grams of aspirin (CgHg04) formed in the reaction of 2.5 grams of salicylic acid (C7H6O3) with excess acetic anhydride and then show the calculation of (2) the % yield if the actual yield of aspirin is 1.89 grams. Reaction is shown below: O. OH соон ООН Acetic Anhydride Salicylic acid ASPRIN Acetylsaicyic acid BACKNE REPORT A PROBLEM All Rights Reserved Design
can you please help me with this !!!
which ever you can is fine, please... thanks !
Results/Data • Aspirin synthesis salicylic acid: 2.0 g Acetic anhydride: 2 mL d= 1.082g/ml sodium acetate: 0.4 g • Experimental yield of aspirin: 2.4 g REPORT DATE: NAME: LAB PARTNER: I PREPARATION OF METHYL SALICYLATE (OIL OF WINTERGREEN): Reaction Odor: Color after addition of FeCl solution: Control Odor: Color after addition of FeCl3 solution: Question Which functional group of salicylic acid forms a...
please help me ! do you think this is good so far ?
Results/Data • Aspirin synthesis salicylic acid: 2.0 g Acetic anhydride: 2 mL d= 1.082g/mL sodium acetate: 0.4 g • Experimental yield of aspirin: 2.4 g FORMATION OF ESTERS II. PREPARATION OF ACETYL SALICYLIC ACID (ASPIRIN): 1 Complete the table below by entering appropriate values into the empty boxes. Show calculations for all entries clearly below. Reactants Chemical MW Grams of Moles of Moles of Limiting Melting Formula...
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