GCMS Data: Briefly discuss how the GC-MS supports the identity of the product. In your discussion of the GC-MS data, include: a) the molecular ion M* and its corresponding m/z value from the spectrum; b) the base peak (i.e. the peak with highest abundance) and its corresponding m/z. Explain how the GC-MS data allow you to tell whether the reaction was successful or not. In your discussion, include things such as (but not limited to): presence of any major impurities,...
I have gotten these wrong a few times when given a reaction bank but, I do not have a reaction bank and would like step by step help with the question below. I attempted a few times but, I am not coming up with the product. I want you to devise a synthetic route for the molecule shown below. Think through the steps, what should you do first and why. Draw your answer, showing each intermediate along the route, so...
how do I fill this out? Gas Chromatography Mass Spectrometry (GC-MS) Data Interpretation Section T Sam T llam T2pm Sam R 11am GC reten- tian time (min) Functional group(s) based on IR bond absorptions Parent radical cation m/z Molecular Degrees formula unsat uration Compound structure and IUPAC name Bolling point "C) carefully draw each fragment structure with the appropriate formal charge. You need only show one resonance form. 57 a cleavage) 43 (a-cleavage) 1.94 aldehyde or ketone CHO I 72...
Could you please explain how do I do these type of questions in general? I have no idea what goes in or out of the reaction and why. Would be nice if you could go in detail to even the most basic things, thank you! B2. Consider the reactions shown below: 1. EtMgBr (excess) diethyl ether Me 2. H20, HCI Ph Et O reagent(s) 10 Me Et " Product 2 Product 1 a) Draw the structure of organic Product 1...
I did an experiment where I synthesized 2-phenyl-2-propanol using the grignard reaction. please help me answer these lab questions Reagents Moles of Reagent 0.00142 moles (0.224 g)bromobenzene 0.00712 mol (0.173 g) 2 mL of THF (n/a moles) tetrahydrofuran 0.00142 mol (0.083g, 0.11mL) acetone, HPLC grade, anh Reagent Name FW 157.75 24.31 n/a 58 Comments Mg powder grind before using must be anhydrous must be anhydrous Pre-Lab Assignment: 1. Determine the volume (mL) of bromobenzene needed for the experiment. Obtain the...
What is answer of #10?? Report: Hydroboration of 1-Methylcyclohexene Mechanism / GC Analysis / Calculations 1. After reviewing the GC and 'H NMR spectra, what is the major product of the reaction? + 3 a. BH: . THF 3 b. 3 H2O2 OH + 3 OH c. NaOH MOH OH racemic racemic major 2. Draw the complete curved arrow mechanism for the reaction to produce the major product, including both the hydroboration and oxidation steps. Repetitive steps need only be...
What is answer of #9??? Help me Report: Hydroboration of 1-Methylcyclohexene Mechanism / GC Analysis / Calculations 1. After reviewing the GC and 'H NMR spectra, what is the major product of the reaction? + 3 a. BH: . THF 3 b. 3 H2O2 OH + 3 OH c. NaOH MOH OH racemic racemic major 2. Draw the complete curved arrow mechanism for the reaction to produce the major product, including both the hydroboration and oxidation steps. Repetitive steps need...
Grignard Reaction with a Ketone: Triphenylmethanol Introduction: The purpose of this lab is to prepare phenylmagnesium bromide, a Grignard reagent, and react it with benzophenone to give triphenylmethanol. Grignard reagents are very reactive and must be synthesized in an environment free of water or any other source of potential proton donor. Once made, the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone, benzophenone. The result is an alkoxide that is then protonated to give...
Experiment . the reduction of bencil (March 2020) Your name Sodium borohydride is a convert recent for the reduction of dehydes and ketones to 1" and 2 alcohols, respectively. The mechanism of the reaction - (below) is straightforward and is driven by boron's affinity for oxygen. In addition, given borohydride's remarkably low reactivity with OH groups under neutral and especially basic conditions, this reaction can be done in alcohol solvents. This means that (unlike LAH or Grignard reactions) no separate...
hello, i need help with the questions in the second photo Experiment 6. the reduction of bencil (March 2020) Your name Sodium borohydride is a convert recent for the reduction of dehydes and ketones to 1" and 2 alcohols, respectively. The mechanism of the reaction (below) is straightforward and is driven by boron's affinity for oxygen. In addition, given borohydride's remarkably low reactivity with OH groups under neutral and especially basic conditions, this reaction can be done in alcohol solvents....