Question

For each spectrum, draw the compound and designate which peaks coordinate to which features on your...

For each spectrum, draw the compound and designate which peaks coordinate to which features on your compound. Include the spectra with your report. How might the aspirin spectra appear if it was not completely purified (ie. if there was left over salicylic acid)?

For each spectrum, draw the compound and designate which peaks coordinate to which features on your compound. Include the spectra with your report. How might the aspirin spectra appear if it was not completely purified (ie. if there was left over salicylic acid)?

1H-NMR spectrum for salicylic acid

13C-NMR spectrum for salicylic acid

IR spectrum for salicylic acid

13C-NMR spectrum for aspirin

1H-NMR spectrum for aspirin

IR spectrum

for aspirin

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Answer #1

sorry i cant provide IR

but you can get in google image

i am providing here only H1 NMR and 13C NMR

first two spectra are for the salicylic acid

second two spectra are for the Asprin

ChemNMR H Estimation 8.04 7.51 OH 11.0 7.62 он 6.98 5.35 PPM Protocol of the H-1 NMR Prediction: Node OH 5.35 OH 11.0 Shift B

ChemNMR 13C Estimation 131.7 121.2 он 113.1 162.2 135.3 он 180 160 140 120 100 80 60 420 PPM

ChemNMR H Estimation Aspirin 8.18 7.76 он 11.0 7.76 7.91 2.28 PPM Protocol of the H-l NMR Prediction: Node Shift Base + Inc.

ChemNMR 13C Estimation 130.7 он 123.9 150.8 134.3 124.4 169.0 20.3 4 PPM Protocol of the C-13 NMR Prediction: Node Shift Base

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