Get the answer of both questions from following image file:
Please help with both questions d and e d. The solubility of salicylic acid in water...
can you please help me with this !!! which ever you can is fine, please... thanks ! Results/Data • Aspirin synthesis salicylic acid: 2.0 g Acetic anhydride: 2 mL d= 1.082g/ml sodium acetate: 0.4 g • Experimental yield of aspirin: 2.4 g REPORT DATE: NAME: LAB PARTNER: I PREPARATION OF METHYL SALICYLATE (OIL OF WINTERGREEN): Reaction Odor: Color after addition of FeCl solution: Control Odor: Color after addition of FeCl3 solution: Question Which functional group of salicylic acid forms a...
Experiment 2: Synthesis of Aspirin (Acetylsalicylic Acid ) 1. How many moles of salicylic acid are there in 1.0 grams of salicylic acid? 2. How many moles of acetic anhydride are there in 3 mL of acetic anhydride? 3. When 1.0g of salicylic acid and 3 mL of acetic anhydride react, DETERMINE which one is the limiting reactant (you can go to General Chemistry if you need help about limiting reagent)? 4. What is phosphoric acid used for in the...
Please show all steps. 17. Essay (20 pts) How many grams of salicylic acid (Mr = 138 g/mol) and sodium salicylate (Mr = 160 g/mol) would you need to generate a 350 mM buffer system in 750 mL of water at pH 3.80? The pKa of salicylic acid is 2.97. What would be the new pH if you titrated this system with 25 mL of 0.1 M HCI?
used. Experimental . Place 2.0 g of salicylic acid in a 125-mL conical flask. 2. Add 4.0 ml (d = 1.08 g/mL; 4.3 g) of acetic anhydride and 6-8 drops of 85% phosphoric acid. 3. Swirl the flask to mix all reagents, and place it in a 70°C water bath. Heat for about 10 minutes. 4. Remove the flask from the water bath and add 2 mL of cold water drop- wise, swirling the flask after each addition, 5. Add...
In the extraction of salicylic acid from water using dichloroethane, a student begins with 2.9 grams of the salicylic acid dissolved in 100 ml of water. After extraction with 20 ml of dichloroethane, drying and evaporation of the organic layer yielded 1.972 grams of salicylic acid. Assuming the student was efficient and did not lose any material, what is the distribution coefficient (Kd) for the system ? let Kd = (concentration in organic solvent) / (concentration in aqueous solvent) a....
Name Section/CRN POST LABORATORY QUESTIONS 1. A student weighs out 3.52 g. of salicylic acid in a 100 ml flask and adds 2.3 mL of acetic anhydride (density 1.080 g/mL). Determine the maximum (theoretical) number of grams of acetylsalicylic acid she can prepare. 2. If the student obtained 4.21 g, of aspirin, calculate the % yield. Briefly, explain why she might have obtained this amount of product. 3. The solubility of Aspirin (acetylsalicylic acid) at 25 °C is 3.0 mg/mL...
please help me ! do you think this is good so far ? Results/Data • Aspirin synthesis salicylic acid: 2.0 g Acetic anhydride: 2 mL d= 1.082g/mL sodium acetate: 0.4 g • Experimental yield of aspirin: 2.4 g FORMATION OF ESTERS II. PREPARATION OF ACETYL SALICYLIC ACID (ASPIRIN): 1 Complete the table below by entering appropriate values into the empty boxes. Show calculations for all entries clearly below. Reactants Chemical MW Grams of Moles of Moles of Limiting Melting Formula...
PREPARATION OF PHARMACEUTICALS - Fischer Esterification Reactions Q: Calculate the expected mass of both methyl salicylate and aspirin assuming 100% yield. EXPERIMENT7 PREPARATION OF PHARMACEUTICALS Fischer Esterification Reactions Almost 2500 years ago, physicians such as Hippocrates recommended that patients chew on the bark of the willow to alleviate pain. The active ingredient in willow bark was found to be salicin, a compound made of a molecule of salicyl alcohol bonded to a p-D-glucose molecule. In the stomach, the bond between...
Question 2 Salicylic acid, HC,H,0, is a chemical compound used in many facial cleansing products. Figure 2. Structure of Salicylic Acid a) Identify the ionizable hydrogen (HA or Hg) with the correct pk НА lonizable Hydrogen pK, 2.97 HA 13.7 :91 3 19- 10 b) The solubility of salicylic acid in water is 0.210-96 HC,HsOs by mass. What is the pH of an aqueous solution of salicylic acid at saturation? (Assume the density of the solution is 1.00 g/mL). 2-U...
QUESTION 3 Salicylic acid reacts with acetic anhydride to form aspirin and acetic acid as shown. Use the equation to answer Questions 3 – 6. (salicylic acid) (aspirin) C7H6O3 (s) + C4H6O3 (l) → C9H8O4 (s) + CH3COOH (l) MM = 138 MM = 180 If we divide 180 by 138 we find that 1.00 g salicylic acid will produce a maximum of 1.30 g aspirin. 3. A student starts with 3.20 g salicylic acid. What is the maximum amount...