Fractionating column
Thermometer
Thermometer adapter
Distilling head
Round-bottom distilling flask
Clamps
Condenser
Water tubing for cooling
Vacuum adapter
Boiling chips/stones/beads
Round-bottom receiving flask
Heating mantle
Beaker for hot water bath
Hot plate
Closed-end capillary tubes (same as used with melting point)
Small or medium test tube
Rubber bands
Reagents
1. Ethanol
2. DI water
Above are the materials and products used in the fractional distillation procedure. Come up with 2 aspects of the protocol that are not green.
Analysing all the elements of the condenser set-up I can only come up with two elements that are not green or that has some hazard associated with them.
1. Thermometers :
Apparently, thermometers are very safe and efficient way to get a track of temperature of a system. But, it contains Mercury (Hg) in it which is extremely hazardous to environment as Hg is the main source of fatal diseases.
2. Rubber band :
Rubber bands apparently looks least harmful of all the elements. But, recycling rubber is very tough process as it stays in the environment and doesn't degrade easily. Moreover, rubber products cause skin irritations, respiratory disorders, etc
Fractionating column Thermometer Thermometer adapter Distilling head Round-bottom distilling flask Clamps Condenser Water tubing for cooling...
Assemble the glassware for fractional distillation according to the diagram and discussion above. Make certain that all joints are secure and that the apparatus is appropriately supported. Remember to allow for space below the distillation flask for the heating mantle and below the receiving flask for an ice bath. Pay extra attention to the positioning of the bulb of the thermometer as mentioned in the introduction. It is critical that the thermometer be positioned correctly for accurate temperature measurement. Using...
Procedure Reaction: Add about 15 mL (measured precisely) of t-amyl alcohol to a 50 mL round bottom flask (the flask will become your stillpot). Cool the pot in an ice-water bath and slowly add, with swirling, about 5 mL of 9 M sulfuric acid. Add two boiling chips then clamp the flask to your ring stand. Do not leave the flask someplace it can be knocked over. Set up a fractional distillation with a foil wrapped Vigreux column. Use a...
Procedure Reaction: Add about 15 mL (measured precisely) of t-amyl alcohol to a 50 mL round bottom flask (the flask will become your stillpot). Cool the pot in an ice-water bath and slowly add, with swirling, about 5 mL of 9 M sulfuric acid. Add two boiling chips then clamp the flask to your ring stand. Do not leave the flask someplace it can be knocked over. Set up a fractional distillation with a foil wrapped Vigreux column. Use a...
answer questions #1-7 and I'll send more information on question #7. We were unable to transcribe this imagesolution of a Mixture by Distillation 4 BACKGROUND s one of the most common methods of purifyinga ery simple method: a liquid is brought to a boil, the liquid becomes a gas the gas a liquid. It is a collected returns to the liquid state and the liquid acquire sufficient e from the liquid phase and enter into the s vapor phase Evaporation...
1. Procedure A. Lithium 2,6-dimethylphenoxide. In a 300-ml. flask, equipped with a magnetic stirrer and a reflux condenser and flushed with nitrogen, are placed 150 ml. of toluene (freshly distilled from sodium), 1.40 g. (0.202 mole) of lithium metal (Note 1) and 25.0 g. (0.205 mole) of resublimed 2,6-dimethylphenol. The mixture is heated under reflux with stirring for 36 hours; a nitrogen atmosphere is maintained for the reflux period (Note 2). The condenser is replaced by a distillation head with...
Give a detailed mechanism for this reaction and give a separation scheme NUCLEOPHILIC ACYL SUBSTITUTION: Synthesis of an Ester Isoamyl acetate (Banana Oil) Purpose This experiment demonstrat and alcohol. The technique of refluxing the reaction mixture is introduced. es the procedure for the synthesis of an ester from a carboxylic acid Esters are an important functional group in organic chemistry, and esters are found widely distributed in nature. Many lower molecular weight esters are associated with natural fuit flavors and...