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Experiment 3 Post-Lab Questions 1. Provided below is the structure of the minor product of the...
3. shown below is the IR spectrum 2-acetylcyclohexanone (the structure is provided in the spectrum). 2-acetylcyclohexanone...
3. shown below is the IR spectrum 2-acetylcyclohexanone (the
structure is provided in the spectrum). 2-acetylcyclohexanone
Exists as an equilibrium mixture of diketone and two enol forms.
Both the diketonr and enol forms can be seen in the provide IR
spectrum although the two different enols cannot be distinguished.
The IR spectra of both enols is essentially identical and so do not
be concerned with distinguishing the enols, just assign peaks to a
"generic" enol.
On the spectrum identify the...
Number 6 and 7. label both spectra of pure p-acetamidophenol and phenacetin product by indicating the...
Number 6 and 7. label both spectra of pure p-acetamidophenol and
phenacetin product by indicating the bonds
5. Spectra 6. Label the IR spectrum of pure p-acetamidophenol below by indicating the bonds associated with stretches in the functional group region. LO0 50 D 000 500 S00 200 3000 4000 7. Label the IR spectrum of your product by indicating the bonds associated with stretches in the functional group region and attach it to Lab report. your % Transmittance 3269.20 3189.76...
1. shown below are IR spectra of cyclohexanecarbaldehyde (I) and cyclohexene (II). which of the spectra...
1. shown below are IR spectra of cyclohexanecarbaldehyde (I)
and cyclohexene (II). which of the spectra A and B corresponds to
which structure (I or II)? On each spectrum identify the peaks that
are associated with a specific bond vibration bond by drawing the
functional group for that bond, circling the specific vibrating
bond and drying and arrow from the circled bond to the absorption
peak. include all the C-H bonds.
2. provided below are IR spectra of
1,2,3,6-tetrahydrobenzaldehyde (I)...
3. (3 pts.) Shown below is the IR spectrum 2-acetylcyclohexanone (the structure is provided in the...
3. (3 pts.) Shown below is the IR spectrum 2-acetylcyclohexanone (the structure is provided in the spectrum). 2- acetylcyclohexanone exists as an equilibrium mixture of diketone and two enol forms. Both the diketone and enol forms can be seen in the provide IR spectrum, although the 2 different enols cannot be distinguished. The IR spectra of both enols is essentially identical and so do not be concerned with distinguishing the enols, just assign peaks to a “generic" enol. On the...
2. (2 pts.) Provided below are IR spectra of 1,2,3,6-tetrahydrobenzaldehyde (I) and 3-methyl-2-cyclohexen-1-one (II). Decide which...
2. (2 pts.) Provided below are IR spectra of 1,2,3,6-tetrahydrobenzaldehyde (I) and 3-methyl-2-cyclohexen-1-one (II). Decide which of the IR spectra A and B corresponds to which structure (I or II). On each spectrum, identify the peaks that are associated with a specific bond vibration bond by drawing the functional group for that bond, circling the specific vibrating bond and drawing an arrow from the circled bond to the absorption peak, as appropriate. Include all the C-H bonds. odo and II...
IR Spectroscopy of Aspirin 1. Draw the structure of aspirin and state the chemical name of...
IR Spectroscopy of Aspirin 1. Draw the structure of aspirin and state the chemical name of aspirin. 2. Indicate the regions (circle and label on your IR spectrum) of your spectrum that correspond to a carbonyl and a hydroxyl functional group. Identify two other regions that correlate with other functional groups/structural features. Indicate these regions on your spectrum (circle and label on your IR spectrum). 3. Use your IR spectrum, melting point data, and FeCly test results to characterize the...
For the reaction below, focus only on 2-methyl-2-butanol (starting material) and 2-chloro-2-methylbutane (desired product). We will...
For the reaction below, focus only on 2-methyl-2-butanol
(starting material) and 2-chloro-2-methylbutane (desired product).
We will not analyze HCl or H2O by IR.
From the two IR spectra below, identify which spectrum belongs
to which molecule. Then label the IR spectrum with the molecule’s
characteristic IR peaks. Highlight or place a box around the most
characteristic peak in the starting material’s IR. You do not need
to label the fingerprint region.
For the reaction below, focus only on 2-methyl-2-butanol...
1. In the H NMR, draw the structure of the molecule directly on the spectrum and...
1. In the H NMR, draw the structure of the molecule directly on
the spectrum and identify each unique proton. Indicate which proton
is responsible for each peak.
2. In the IR spectrum, indicate which functional group is
responsible for each important peak. Attempt to identify at least
five important peaks. In you discussion, indicate which peaks are
most helpful in determining whether or not you converted the
starting material to the desired product.
3. Compare the IR spectrum of...
identify the peaks above 1500 cm-1 with the corresponding functional groups Lab Information fo... X Methyl...
identify the peaks above 1500 cm-1 with the corresponding
functional groups
Lab Information fo... X Methyl benzoate: 105.0 SN 1491. 1912.13 160135 MIN At 9 .49 22.00 1919 1452b0 1315 14 1176.17 143475 26.50 7007 0.0 4000.0 3000 2000 1500 cm-1 1000 650.0 Postlab instructions and supplemental questions: 1) Calculate your percent yield of methyl benzoate based on the data provided. 2) For all three products obtained, tabulate all peaks above 1500 cm, and the most substantial peak below 1500...
Tools Window Help OMX 75% Esterification Experiment Lab Data.pdf (page 1 of 3) Search Product Ester...
Tools Window Help OMX 75% Esterification Experiment Lab Data.pdf (page 1 of 3) Search Product Ester IR of starting alcohol (1-pentanol) 1-Pentanol M. AM 19ra aromo 14, 2017 m. 1% 1075 20 . 2030 26.1.60.39 10 4000 3500 . 1000 3000 INT 650 2500 cm-1 2000 1500 M 8 Tools Window Help 78 Wed 2:19 PM Go Esterification Experiment Lab Data pdf page 2 of 3) @ Q Search IR of final product (ester) Product Ester Guided Instructions for In-Lab...
3. shown below is the IR spectrum 2-acetylcyclohexanone (the
structure is provided in the spectrum). 2-acetylcyclohexanone
Exists as an equilibrium mixture of diketone and two enol forms.
Both the diketonr and enol forms can be seen in the provide IR
spectrum although the two different enols cannot be distinguished.
The IR spectra of both enols is essentially identical and so do not
be concerned with distinguishing the enols, just assign peaks to a
"generic" enol.
On the spectrum identify the...
Number 6 and 7. label both spectra of pure p-acetamidophenol and
phenacetin product by indicating the bonds
5. Spectra 6. Label the IR spectrum of pure p-acetamidophenol below by indicating the bonds associated with stretches in the functional group region. LO0 50 D 000 500 S00 200 3000 4000 7. Label the IR spectrum of your product by indicating the bonds associated with stretches in the functional group region and attach it to Lab report. your % Transmittance 3269.20 3189.76...
1. shown below are IR spectra of cyclohexanecarbaldehyde (I)
and cyclohexene (II). which of the spectra A and B corresponds to
which structure (I or II)? On each spectrum identify the peaks that
are associated with a specific bond vibration bond by drawing the
functional group for that bond, circling the specific vibrating
bond and drying and arrow from the circled bond to the absorption
peak. include all the C-H bonds.
2. provided below are IR spectra of
1,2,3,6-tetrahydrobenzaldehyde (I)...
3. (3 pts.) Shown below is the IR spectrum 2-acetylcyclohexanone (the structure is provided in the spectrum). 2- acetylcyclohexanone exists as an equilibrium mixture of diketone and two enol forms. Both the diketone and enol forms can be seen in the provide IR spectrum, although the 2 different enols cannot be distinguished. The IR spectra of both enols is essentially identical and so do not be concerned with distinguishing the enols, just assign peaks to a “generic" enol. On the...
2. (2 pts.) Provided below are IR spectra of 1,2,3,6-tetrahydrobenzaldehyde (I) and 3-methyl-2-cyclohexen-1-one (II). Decide which of the IR spectra A and B corresponds to which structure (I or II). On each spectrum, identify the peaks that are associated with a specific bond vibration bond by drawing the functional group for that bond, circling the specific vibrating bond and drawing an arrow from the circled bond to the absorption peak, as appropriate. Include all the C-H bonds. odo and II...
IR Spectroscopy of Aspirin 1. Draw the structure of aspirin and state the chemical name of aspirin. 2. Indicate the regions (circle and label on your IR spectrum) of your spectrum that correspond to a carbonyl and a hydroxyl functional group. Identify two other regions that correlate with other functional groups/structural features. Indicate these regions on your spectrum (circle and label on your IR spectrum). 3. Use your IR spectrum, melting point data, and FeCly test results to characterize the...
For the reaction below, focus only on 2-methyl-2-butanol
(starting material) and 2-chloro-2-methylbutane (desired product).
We will not analyze HCl or H2O by IR.
From the two IR spectra below, identify which spectrum belongs
to which molecule. Then label the IR spectrum with the molecule’s
characteristic IR peaks. Highlight or place a box around the most
characteristic peak in the starting material’s IR. You do not need
to label the fingerprint region.
For the reaction below, focus only on 2-methyl-2-butanol...
1. In the H NMR, draw the structure of the molecule directly on
the spectrum and identify each unique proton. Indicate which proton
is responsible for each peak.
2. In the IR spectrum, indicate which functional group is
responsible for each important peak. Attempt to identify at least
five important peaks. In you discussion, indicate which peaks are
most helpful in determining whether or not you converted the
starting material to the desired product.
3. Compare the IR spectrum of...
identify the peaks above 1500 cm-1 with the corresponding
functional groups
Lab Information fo... X Methyl benzoate: 105.0 SN 1491. 1912.13 160135 MIN At 9 .49 22.00 1919 1452b0 1315 14 1176.17 143475 26.50 7007 0.0 4000.0 3000 2000 1500 cm-1 1000 650.0 Postlab instructions and supplemental questions: 1) Calculate your percent yield of methyl benzoate based on the data provided. 2) For all three products obtained, tabulate all peaks above 1500 cm, and the most substantial peak below 1500...
Tools Window Help OMX 75% Esterification Experiment Lab Data.pdf (page 1 of 3) Search Product Ester IR of starting alcohol (1-pentanol) 1-Pentanol M. AM 19ra aromo 14, 2017 m. 1% 1075 20 . 2030 26.1.60.39 10 4000 3500 . 1000 3000 INT 650 2500 cm-1 2000 1500 M 8 Tools Window Help 78 Wed 2:19 PM Go Esterification Experiment Lab Data pdf page 2 of 3) @ Q Search IR of final product (ester) Product Ester Guided Instructions for In-Lab...
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