i need help answering the questions plz and thanks! Experiment 9 Report Sheet: Calculations and Questions...
i need to calculate the theortetical yield by finding the limiting reactant of the experiment by converting reactants to product, then calculate the percent yield using the limiting reactant -in my experiment the amout of crystals i obtained was 1.232 g (watch glass + filter paper = 31.228 g and watch glass, filter paper, + crystals = 32.460 g) REACTION SCHEME H сно, ОН- ОСH, CH panisaldehyde acetophenone Molar Mass: 120.15g/mol Molar Mass: 136.15g/mol Molar Mass: 239.30g/mol Density: 1.119g/mL Density:...
Please help! (These are the instructions I had) 1) Preparation of K2[Cu(C2O4)2] 2H2O CuSO4•5H2O + 2K2C2O4•H2O → K2[Cu(C2O4)2]•2H2O + K2SO4 + 5H2O Heat a solution of 2.5g of potassium oxalate monohydrate in 12.5mL of water contained in a 50mL beaker (approx. 90°C). Heat 1.55g of copper sulfate pentahydrate in 3mL of water to about 90°C and add it rapidly, with vigorous stirring to the hot potassium oxalate solution. Set on the bench and allow to cool to room temperature then...
SYNTHESIS OF trans-p-ANISALACETOPHENONE Prepare a table of all chemicals used in the procedure with their purpose Melting point of trans-p-anisalacetophenone (with source) and Molar mass of trans-p-anisalacetophenone (with source) (i cant find these two things anywhere) Procedure: 1. Carefully measure 1.0 mL each of p-anisaldehyde and acetophenone and place them in a screw-cap testtube. 2. To this add 3.0 mL of 95% ethanol. Shake the test tube gently to achieve a homogenous mixture. 3. Add 6-7 drops of 40% sodium...
The first picture is used for question #2, and question #3 can be normally answered. I believe the answer to question 3 is -> 0.07144M. However I would like someone to check it. I am not sure about 2. BE SURE THAT YOU RECORD ALL OF YOUR DATA AND LABEL PROPERLY FOR PARTI OF THIS LABORATORY EXPERIMENT. YOU WILL NEED TO ACCESS THIS INFORMATION IN THREE WEEKS. Part I Synthesis of the Complex Salt containing Copper Procedure 16.004 1. In...
Heat lamp or drying oven Hydrated copper chloride Distilled water Aluminum wire 30-ml beaker Glass rod Watch glass Buchner fiannel Hot plate Ethanol Füter paper CAUTION: Wear all safety equipment, follow all normal safety procedures and experiment as directed by your instructor follow instructions. Dispose of all liquid AND solid waste products from the 1. Weigh a clean, dry 30-mL beaker and record its mass to 3 decimal places. When-it-is-time,heat the beaker 2. Add approximately 1.00 gram of the hydrated...
1.) What side reactions occur during the following steps. 2.) How can the IR spectrum be used to show that there is not starting material left and the products are ketones? 3.) Describe the major differences and similarities between the IR spectra of benzoin and benzil. Compare your IR spectrum with those of benzoin and benzil. Copper-Catalyzed Oxidation of Benzoin 1. Add a stir bar and 1.5 mL of glacial acetic acid, 0.250 g of NH4NO3 and 0.500 g of...
Write out your separation scheme for this experiment. 1. Heat 75 mL of water to 90 °C in a 250-mL beaker. 2. While the water is being heated, place 250 mg of salicylic acid, 1 drop of 85% phosphoric acid and 0.5 mL of acetic anhydride in a test tube. Add a boiling chip to the mixture and gently shake it in order to mix the reactants. 3. Heat the tube in the beaker of water at 85 - 90...
THE EMPIRICAL FORMULA OF SELECTED HYDRATES experiment PROCEDURE THIS EXPERIMENT SHOULD BE DONE IN PAIRS. 1. Available to you should be: a Büchner funnel, a rubber funnel adapter, side-arm filter flask, thick-walled rubber tubing, plastic forceps and a plastic spatula. 2. Before you turn the hotplate on, wipe the hotplate down with a damp paper towel. During this experiment you will be placing filter paper containing products directly onto the surface of the hotplate. As such, you will want to...
3. Crystallization begins with a process called nucleation, where particles of the substance dissolved in solution begin to aggregate. Crystals then begin to form on these aggregates. Based on this, explain why Steps 3 and 4 in Part III may induce crystallization. Part II: Observations Upuy Describe qualitative changes to solution - Solution went from bright yellow, orange to a mare dacu Orange /ced - hydrogen peroxide is originally clear but tuck's oldcu in the solution. The addition of hydrogen...
Determine the theoretical yield and limiting reagent Running the Reaction Add 0.100 g benzil and 0.30 mL 95% ethanol to a 3-mL conical vial. Place a spin vane in the vial and attach an air condenser. Heat the mixture with an aluminum block (90-100°C) while stirring until the benzil has dissolved (see inset in Tech- nique 6, Figure 6.1A). Using a 9-inch Pasteur pipette, add dropwise 0.25 mL of an aqueous potassium hydroxide solution' downward through the condenser into the...