LAB Using a mortar and pestle, grind approximately 5 g of sodium hydroxide into fine particles....
LAB
- Using a mortar and pestle, grind approximately 5 g of sodium hydroxide into fine particles.
- Add 0.50 g of 3,4-dimethoxybenzaldehyde and 0.40 g of 1-indanone to a test tube.
- Using a vortex mixer, gently mix the two solids together, forming an oil.
- Add 0.10 g of finely ground sodium hydroxide from Step 1 to the oil.
- Allow the reaction to sit for 15 minutes.
- Add 4 mL of 10% aqueous hydrochloric acid.
- Isolate the product by vacuum filtration.
- Recrystallize the product using 90% aqueous ethanol. The recrystallization should require between 30–40 mL of solvent.
- Obtain the melting point of the product.
A. What should be the order of combining the 3 reactants, if each of the reacting compounds were dissolved in solvent?
B. What reaction can happen if the chemicals were added in the wrong order?
Homework Answers
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LAB
Using a mortar and pestle, grind approximately 5 g of sodium
hydroxide into fine particles....
Why is the benzaldehyde preferentially attacked by the 1-indanone over another 1-indanone? Using a mortar and...
Why is the benzaldehyde preferentially attacked by the 1-indanone over another 1-indanone? Using a mortar and pestle, grind approximately 5 g of sodium hydroxide into fine particles. Add 0.50 g of 3,4-dimethoxybenzaldehyde and 0.40 g of 1-indanone to a test tube. Using a vortex mixer, gently mix the two solids together, forming an oil. Add 0.10 g of finely ground sodium hydroxide from Step 1 to the oil. Allow the reaction to sit for 15 minutes. Add 4 mL of...
tthe weight of my product is 0.87 g and they gave me the density! how can...
tthe weight of my product is 0.87 g and they gave me the
density! how can i calculte the percent yield?
- Page < 8 > of 14 | 0 Data and Observations Weight of product: Melting range of product: Attach any spectra to your laboratory report Calculations and Graphs Calculate the percent yield. Keep in mind that the reagents may not be 100% pure; refer to labels on the containers. The density of 50% aqueous sodium hydroxide is 1.5...
I need help calculating theoretical yield for my Diels-Alder lab experiment. This reaction was between 1,3-butadiene...
I need help calculating theoretical yield for my
Diels-Alder lab experiment. This reaction was between 1,3-butadiene
and maleic anhydride, forming cis 1,2,3,6-tetrahydrophthalic
anhydride. In this experiment 1.0g of maleic anhydride was combined
with 1.8g 3-sulfolene and 2 mL dry xylene and refluxed for 30 mins.
6 mL of xylene was added to dissolve solids and then decanted, then
warm pet. ether was added to form crystalline product after
cooling. some of this info may be irrelevant in what is needed...
Lab : Aldol Condensation Purpose. In this lab you will conduct the Aldol condensation reaction under solid-state...
Lab : Aldol Condensation Purpose. In this lab you will conduct the Aldol condensation reaction under solid-state reaction conditions that will involve grinding reactants in the solid phase. You must read ahead and learn about this reaction and the chemical mechanism for the Aldol condensation. There are two possible products which are the initial Aldol or subsequent elimination product. You will need to isolate and purify your reaction product. You will use your melting point, IR, 1H and 13C NMR spectra to...
After I made extraction I put dry agent ( sodium magniusm) and the lab time is...
After I made extraction I put dry agent ( sodium magniusm) and
the lab time is up and I left it for two days insteaf of 10 mins
and all my product is gone
Can you pease think if reasons why nothing left ?
Dissolve 12.5 g (0.103 mole) recovered amine, [α]D27: +24.50, in 88 ml of 95% ethanol. (This solution contains 0.062 mole excess +)-amine, based on [a]D2: +40.7° for the pure (+)-amine, and 0.041 mole racemic amine Heat...
What is the reaction product(s) of oleic acid & sodium methoxide? Show the structure(s). Part A:...
What is the reaction product(s) of oleic acid & sodium methoxide? Show the structure(s). Part A: Acid Catalyzed Fischer Esterification of Free Fatty Acids Add 20 mL of canola oil and a magnetic stir bar to a 125-mL Erlenmeyer flask, and place the flask on a magnetic stirring plate. Add 2–3 mL of methanol and up to three drops of concentrated sulfuric acid Perform this step with caution, as this is a strong acid! Immerse a thermometer into the reaction...
what is the theoretical yield of anisalacetophenone and dibenzalacetone formed? thank you. The Aldol Condensation Precautions:...
what is the theoretical yield of anisalacetophenone and
dibenzalacetone formed? thank you.
The Aldol Condensation Precautions: Acetone, ethanol and acetophenone are flammable; work in a fume hood. Sodium hydroxide is a strong base and can cause severe skin burns and eye damage. Safety goggles are required. Gloves are recommended. Purpose To carry out two Aldol condensation reactions in which no heat is needed to obtain the condensation product. The two reactions differ in the number of enolizable protons at the...
Questions and Exercises 1. In the course of reflux of the triglyceride in a sodium hydroxide solu...
Organic Chemistry Help!
Questions and Exercises 1. In the course of reflux of the triglyceride in a sodium hydroxide solution you will notice a lot of foaming. Explain. What is left behind in the aqueous layer after filtration of the saponification product? The starting material and the product of the saponification reaction have similar melting points. How do you know you actually isolated a new product rather than just recovered the starting material? Give at least two different methods to...
i need to calculate the theortetical yield by finding the limiting reactant of the experiment by...
i need to calculate the theortetical yield by finding the
limiting reactant of the experiment by converting reactants to
product, then calculate the percent yield using the limiting
reactant
-in my experiment the amout of crystals i obtained was 1.232 g
(watch glass + filter paper = 31.228 g and watch glass, filter
paper, + crystals = 32.460 g)
REACTION SCHEME H сно, ОН- ОСH, CH panisaldehyde acetophenone Molar Mass: 120.15g/mol Molar Mass: 136.15g/mol Molar Mass: 239.30g/mol Density: 1.119g/mL Density:...
SYNTHESIS OF trans-p-ANISALACETOPHENONE Prepare a table of all chemicals used in the procedure with their purpose...
SYNTHESIS OF trans-p-ANISALACETOPHENONE
Prepare a table of all chemicals used in the procedure with
their purpose
Melting point of trans-p-anisalacetophenone (with source) and
Molar mass of trans-p-anisalacetophenone (with source) (i cant find
these two things anywhere)
Procedure: 1. Carefully measure 1.0 mL each of p-anisaldehyde and acetophenone and place them in a screw-cap testtube. 2. To this add 3.0 mL of 95% ethanol. Shake the test tube gently to achieve a homogenous mixture. 3. Add 6-7 drops of 40% sodium...
tthe weight of my product is 0.87 g and they gave me the
density! how can i calculte the percent yield?
- Page < 8 > of 14 | 0 Data and Observations Weight of product: Melting range of product: Attach any spectra to your laboratory report Calculations and Graphs Calculate the percent yield. Keep in mind that the reagents may not be 100% pure; refer to labels on the containers. The density of 50% aqueous sodium hydroxide is 1.5...
I need help calculating theoretical yield for my
Diels-Alder lab experiment. This reaction was between 1,3-butadiene
and maleic anhydride, forming cis 1,2,3,6-tetrahydrophthalic
anhydride. In this experiment 1.0g of maleic anhydride was combined
with 1.8g 3-sulfolene and 2 mL dry xylene and refluxed for 30 mins.
6 mL of xylene was added to dissolve solids and then decanted, then
warm pet. ether was added to form crystalline product after
cooling. some of this info may be irrelevant in what is needed...
After I made extraction I put dry agent ( sodium magniusm) and
the lab time is up and I left it for two days insteaf of 10 mins
and all my product is gone
Can you pease think if reasons why nothing left ?
Dissolve 12.5 g (0.103 mole) recovered amine, [α]D27: +24.50, in 88 ml of 95% ethanol. (This solution contains 0.062 mole excess +)-amine, based on [a]D2: +40.7° for the pure (+)-amine, and 0.041 mole racemic amine Heat...
what is the theoretical yield of anisalacetophenone and
dibenzalacetone formed? thank you.
The Aldol Condensation Precautions: Acetone, ethanol and acetophenone are flammable; work in a fume hood. Sodium hydroxide is a strong base and can cause severe skin burns and eye damage. Safety goggles are required. Gloves are recommended. Purpose To carry out two Aldol condensation reactions in which no heat is needed to obtain the condensation product. The two reactions differ in the number of enolizable protons at the...
Organic Chemistry Help!
Questions and Exercises 1. In the course of reflux of the triglyceride in a sodium hydroxide solution you will notice a lot of foaming. Explain. What is left behind in the aqueous layer after filtration of the saponification product? The starting material and the product of the saponification reaction have similar melting points. How do you know you actually isolated a new product rather than just recovered the starting material? Give at least two different methods to...
i need to calculate the theortetical yield by finding the
limiting reactant of the experiment by converting reactants to
product, then calculate the percent yield using the limiting
reactant
-in my experiment the amout of crystals i obtained was 1.232 g
(watch glass + filter paper = 31.228 g and watch glass, filter
paper, + crystals = 32.460 g)
REACTION SCHEME H сно, ОН- ОСH, CH panisaldehyde acetophenone Molar Mass: 120.15g/mol Molar Mass: 136.15g/mol Molar Mass: 239.30g/mol Density: 1.119g/mL Density:...
SYNTHESIS OF trans-p-ANISALACETOPHENONE
Prepare a table of all chemicals used in the procedure with
their purpose
Melting point of trans-p-anisalacetophenone (with source) and
Molar mass of trans-p-anisalacetophenone (with source) (i cant find
these two things anywhere)
Procedure: 1. Carefully measure 1.0 mL each of p-anisaldehyde and acetophenone and place them in a screw-cap testtube. 2. To this add 3.0 mL of 95% ethanol. Shake the test tube gently to achieve a homogenous mixture. 3. Add 6-7 drops of 40% sodium...
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