1.a IR spectroscopy and Thin Layer Chromatography (TLC) is very convenient in tracking reactions. Explain How...
1.a
IR spectroscopy and Thin Layer Chromatography (TLC) is very convenient in tracking reactions. Explain How you used both IR and TLC to track your reaction. Was your reaction complete when you did your initial TLC check? If so, how can you tell?
1.b
Discuss how yield can be correlated to the efficacy of a reaction? Why are yields never 100%?
Homework Answers
Add Answer to:
1.a
IR spectroscopy and Thin Layer Chromatography (TLC) is very
convenient in tracking reactions. Explain How...
Can you help me answer the questions for the Introduction/Background? 1. Introduced the techniques of thin-layer...
Can you help me answer the questions for the
Introduction/Background?
1. Introduced the techniques of thin-layer and flask column
chromatography. Discuss how a solvent is elected as eluent.
2. Discuss all the applications of TLC. What is it used for?
3. Discuss the mobile and stationary phases of TLC and column
chromatography.
4. Explain how column chromatography can be used to separate a
mixture on a larger scale than TLC.
Post-Lab: Objective State the objective of the experiment in your...
1. What is the purpose of Thin-Layer Chromatography (TLC)? 2. What are the phases involved in...
1. What is the purpose of Thin-Layer Chromatography (TLC)? 2. What are the phases involved in TLC? 3. What is coated on the TLC plate? 4. What is the purpose of lining the wall of the TLC chamber with paper? 5. Why is it important to use a small amount of the mobile phase? 6. Why should you remove the TLC plate before the mobile phase reaches the top? 7. What type of compounds are visible with UV light? 8....
Wanting to monitor the reaction progress you decide to use normal phase thin-layer chromatography, but do...
Wanting to monitor the reaction progress you decide to use normal phase thin-layer chromatography, but do not know what the best conditions are to use. If you had the standards for all potential products and your starting materials, outline how would you go about determining the best TLC conditions for monitoring the reaction progress. Provide drawings of an ideal TLC plate with the number of theoretical products you would expect and their relative positions. How do you know when the...
Laboratory Instructor STUDENT REPORT A. Data Sheet EXPERIMENT 28 Aspartame 1. Thin-layer chromatography Distance traveled by...
Laboratory Instructor STUDENT REPORT A. Data Sheet EXPERIMENT 28 Aspartame 1. Thin-layer chromatography Distance traveled by solvent (1) Substance Distance teweled DR value Calculations: 2. KMnO, test Observations 10 min. 15 min. Reaction? 5 min. Substance 1092 330 Exploring Chemistry 3. Cari nitrate test B. Reflective Exercises and phenylalanine columns on the 1. How many spots should be seen for each of the aspartic acid and price chromatogram? Why? 2. Referring to the chromatogram, what did you here and what...
QUESTIONS 1. In your own words, explain how the components of a mixture are separated during...
QUESTIONS 1. In your own words, explain how the components of a mixture are separated during thin layer chromatography. Do not explain how to perform TLC; in other words do not explain the procedure. 2. Explain the purpose of the UV lamp in this experiment. 3. Why must you use pencil, not pen, when you make marks on the TLC plate? How do you know? Be sure to 4. Which substances were in the OTC pain reliever? discuss your Rr...
Explain (in your own chemically accurate words) why and how you can use IR spectroscopy to...
Explain (in your own chemically accurate words) why and how you can use IR spectroscopy to measure bonding parameters for a polar, diatomic molecule. You will need to address why the ro-vibrational spectrum is in the IR region of the electromagnetic spectrum (this may include a discussion of vibrational and rotational motion and the selection rules associated with them) the origin of the P, Q and R branch (including a figure to indicate the origin of each set of peaks...
1151 VCL 11-8: Claisen Condensation -1 For this assignment, the target compound that you should s...
1151 VCL 11-8: Claisen Condensation -1 For this assignment, the target compound that you should synthesize is methyl acetoacetate. This is another carbonyl addition variation. Examine the product and determine which ester is the nucleophile and which is the electrophile. Keep in mind the mechanism and that you need to acidify the intermediate in order to isolate a neutral product. Synthesis Procedures 1. Start Virtual ChemLab and select Claisen Condensation-I from the list of assignments in the electronic workbook. After...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
QUESTIONS TO ANSWER: Prepare a table of all chemicals used with the structure and purpose of...
QUESTIONS TO ANSWER:
Prepare a table of all chemicals used with the structure and
purpose of each.
Calculate the theoretical yield by finding limiting reactant of
the experiment by converting reactants to product (remember to show
all calculations used)
Calculate the percent yield using the limiting reactant
Calculate the Rf for triphenylmethanol. If there are two dots,
determine which one is triphenylmethanol.. ( I did not provide
data. Please let me know how I Would do this if I did)...
Need help, numbers 3-6 please show work. and fill out table of chemicals for all chemical...
Need help, numbers 3-6 please show work. and fill out table of
chemicals for all chemical used.
calculate mmol in the table as well show work please
and each of these must be listed in its own row. There are 10 column headings: IUPAC name OR common name, structure, CAS number (Chemical Abstract Service number) molecular mass, melting point (if applicable), boiling point (if applicable), solubility (in water, if applicable), density, amounts to be used in the experiment, and the...
Can you help me answer the questions for the
Introduction/Background?
1. Introduced the techniques of thin-layer and flask column
chromatography. Discuss how a solvent is elected as eluent.
2. Discuss all the applications of TLC. What is it used for?
3. Discuss the mobile and stationary phases of TLC and column
chromatography.
4. Explain how column chromatography can be used to separate a
mixture on a larger scale than TLC.
Post-Lab: Objective State the objective of the experiment in your...
1. What is the purpose of Thin-Layer Chromatography (TLC)? 2. What are the phases involved in TLC? 3. What is coated on the TLC plate? 4. What is the purpose of lining the wall of the TLC chamber with paper? 5. Why is it important to use a small amount of the mobile phase? 6. Why should you remove the TLC plate before the mobile phase reaches the top? 7. What type of compounds are visible with UV light? 8....
Laboratory Instructor STUDENT REPORT A. Data Sheet EXPERIMENT 28 Aspartame 1. Thin-layer chromatography Distance traveled by solvent (1) Substance Distance teweled DR value Calculations: 2. KMnO, test Observations 10 min. 15 min. Reaction? 5 min. Substance 1092 330 Exploring Chemistry 3. Cari nitrate test B. Reflective Exercises and phenylalanine columns on the 1. How many spots should be seen for each of the aspartic acid and price chromatogram? Why? 2. Referring to the chromatogram, what did you here and what...
QUESTIONS 1. In your own words, explain how the components of a mixture are separated during thin layer chromatography. Do not explain how to perform TLC; in other words do not explain the procedure. 2. Explain the purpose of the UV lamp in this experiment. 3. Why must you use pencil, not pen, when you make marks on the TLC plate? How do you know? Be sure to 4. Which substances were in the OTC pain reliever? discuss your Rr...
1151 VCL 11-8: Claisen Condensation -1 For this assignment, the target compound that you should synthesize is methyl acetoacetate. This is another carbonyl addition variation. Examine the product and determine which ester is the nucleophile and which is the electrophile. Keep in mind the mechanism and that you need to acidify the intermediate in order to isolate a neutral product. Synthesis Procedures 1. Start Virtual ChemLab and select Claisen Condensation-I from the list of assignments in the electronic workbook. After...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
QUESTIONS TO ANSWER:
Prepare a table of all chemicals used with the structure and
purpose of each.
Calculate the theoretical yield by finding limiting reactant of
the experiment by converting reactants to product (remember to show
all calculations used)
Calculate the percent yield using the limiting reactant
Calculate the Rf for triphenylmethanol. If there are two dots,
determine which one is triphenylmethanol.. ( I did not provide
data. Please let me know how I Would do this if I did)...
Need help, numbers 3-6 please show work. and fill out table of
chemicals for all chemical used.
calculate mmol in the table as well show work please
and each of these must be listed in its own row. There are 10 column headings: IUPAC name OR common name, structure, CAS number (Chemical Abstract Service number) molecular mass, melting point (if applicable), boiling point (if applicable), solubility (in water, if applicable), density, amounts to be used in the experiment, and the...
Most questions answered within 3 hours.
-
You have to write your code in C++ (as a cpp file) and prepare a
docx...
asked 49 minutes ago -
Why does the spectrum of bromocresol green changes at different
pHs? What causes the change?
asked 54 minutes ago -
Rice Company has a unit selling price of $690, variable costs
per unit of $390, and...
asked 1 hour ago -
The DeVille Company reported pretax accounting
income on its income statement as follows:
2018
$
425,000...
asked 1 hour ago -
Argue for or against the "Three Strikes"laws. Provide a rationale
to support your response.
asked 2 hours ago -
Bargaining Models: what is the "Obsolescing Bargain"?
Bargaining Models: what are the factors that would tend...
asked 3 hours ago -
1. A ball is thrown up into the air.
a) Draw motion diagram and the point-like...
asked 3 hours ago -
1) Because money eliminates the "double coincidence of wants"
problem, the development of money as a...
asked 4 hours ago -
Company AAA produces only one product which other manufacturers
purchase as a component for their final...
asked 6 hours ago -
An
item can be appended to an array-based list, provided the lenght is
less than the...
asked 6 hours ago -
Two particles each have a rest mass energy of 30 MeV and are
traveling with a...
asked 8 hours ago -
why
is vectorization a faster alternative to loops?
asked 9 hours ago