What is the theorectical yeild for step 1 and step 3? - Step 1 has 0.76g...
Multistep Synthesis: Synthesis of Amine (Organic Chemistry Lab) Question 1. Explain each step of reaction mechanism. (How does it work?) 2. Discuss reason for reaction sequence. (Why must one reaction occur before another?) 3. Explain how IR supports the major product. Experiment Procedure Imine Formation: Weigh a 20 mL beaker and then add 380 mg of ortho-vanillin and 268 mg of para-toluidine. Care should be taken to add equivalent molar amounts of the two reactants. Observe the mixture and record...
i did the synthesis of aspirin experiment and got the data below. how do you do the theoretical yield? percent yield of the pure aspirin? DATA: Mass of Salicylic Acid: 2.034g Volume of Acetic Anhydride used in synthesis: 4.00ml Mass of filter paper: 0.196g Mass of filter paper plus Aspirin: 1.868g Mass of Aspirin: 1.672g Percent Yield of Pure Aspirin: I Experimental Procedure HAZARD: Sulfuric acid, acetic anhydride and glacial acetic acid are corrosive to the skin. They are also...
use the numbers from image 2 to help me answer all parts from image 1. I am confused how to solve. will rate well 1. The molecular weight of vanillin (a solid) is 152.15. The molecular weight of acetic anhydride (a liquid) is 102.04 and its density is 1.082 g/mL. How many mmoles of vanillin and how many mmoles of acetic anhydride are being reacted in the BASE CATALYZED reaction as described in the textbook? a. 1.97 mmol of vanillin...
for this experiment of syntheis of aspirin, was the product obtained pure (based on color)? how do you know? the color was white Experimental Procedure HAZARD: Sulfuric acid, acetic anhydride and glacial acetic acid are corrosive to the skin. They are also irritants, and all operations in which these substances are used should be carried out under the hood. Prepare a hot-water bath by heating a 400-ml beaker containing about 200 mL of water. 1. Use a centigram balance and...
Question1: Introduction Three aromatic compounds that have ortho-para directing and activating substituents will be brominated. The extent of activation will be judged by the number of bromine atoms that add to the benzene ring in each case. For each of the compounds shown below you will work out if a mono- di- or tri- brominated derivative formed following treatment with acetic acid and bromine in hydrobromic acid. This will be determined by measuring the melting point and interpreting the H...
What is the purpose of extracting the aqueous layer two more times with ether in step 5? What is the purpose of washing the combined organic layers with NaOH in step 6? Thank you Reaction 1: Nitration HNO3 NO2 + H2SO4, H20 NO2 toluene NO2 ortho meta para Procedure for Reaction 1: 1) To a stirred solution of 3 ml (44.7 mmoles) 67 % HNO3 in 3.75 mL of water, H2SO4 (9 mL) was slowly added at 10-15 °C. 2)...
1.) What side reactions occur during the following steps. 2.) How can the IR spectrum be used to show that there is not starting material left and the products are ketones? 3.) Describe the major differences and similarities between the IR spectra of benzoin and benzil. Compare your IR spectrum with those of benzoin and benzil. Copper-Catalyzed Oxidation of Benzoin 1. Add a stir bar and 1.5 mL of glacial acetic acid, 0.250 g of NH4NO3 and 0.500 g of...
Can someone tell me if a theoretical yield needs to be calculated for this experiment? And if so, how do you calculate it? please show all work. thank you. btw the aniline weighs 6.69g. Synthesis of Acetanilide Acetanilide is synthesized from aniline by a reaction known as acylation. Acylation is the addition of an acyl group to a compound. In this experiment, aniline (1 amine) is reacted with acetic anhydride (acylating agent) to form acetanilide (an amide). H-C-CH3 + CH...
can someone please answer number one? im so lost DYES AND DYEING CHAPTER 1. Calculate the amounts of salicylic acid, 1-naphthol, 2-naphthol, 8-anilino-1-naph- thalenesulfonic acid ammonium salt, or N,N-dimethylaniline needed for Part 1B of this experiment (use molecules as assigned by your TA). 190mg 3-aminobenzene 2.5mL Sulfonic acid 2.5% sodium carbonate solution 81mg Sodium nitrate 2. What is the purpose of the sodium carbonate in Part 1A? Why do we add glacial acetic acid in Part 13 when we react...
3) The hydrogen atom in HCl is electrophilic whereas the hydrogen atoms in sodium borohydride are nucleophilic. Offer a plausible rationale for this difference in reactivity. PROCEDURES 1. Add 2.00 g of 3-dimethylaminopropiophenone hydrochloride, 10 mL of distilled water and a magnetic stir bar to a 100 ml beaker, and stir to dissolve. This is the reaction beaker. 2. Add (with stirring) sufficient 10% NaOH (about 5-6 mL) to bring the solution to pH > 10. The free base will...