I understand that equivalents is the ratio of the # of moles of a reactant or...
noinizdle dn Draw a flow sheet to describe the separation procedure. (10 pts) doprleoudenagne aded 6. Are several small-scale extractions more efficient than one large-scale extraction? Why? (10 pts) 7. Why the upper layer should be poured out from the top of the separatory funnel but not be drained from the stopcock? (10 pts) Extraction: Separation of a Neutral and Basic Substances 1 Dissolve 2 g of a mixture of naphthalene and 4-chloroaniline in 20 mL of ethyl ether and...
For the nitration of methyl benzoate: a. Which product did you get? What evidence do you have for this? b. Was your product pure? What evidence do you have for this? Explain your evidence. c. Draw the mechanism for the product you got. For the bromination of acetanilide: a. Which product did you get? What evidence do you have for this? b. Was your product pure? What evidence do you have for this? Explain your evidence. c. Draw the mechanism...
complete the stoichiometry table for the process above Experimental Notes 4, H ОН NaBH4 NaOH OH H2O OH Step 1: Procedure for the Sodium Borohydride Reduction of 3-Ethoxy-4-hydroxybenzaldehyde: Dissolve 1.62 g of 3-ethoxy-4-hydroxybenzaldehyde in 10 mL of 1.0 M NaOH in a 125 mL Erlenmeyer flask with a magnetic stir bar. Cool the flask in a cold-water bath, and then add, in small portions, 0.30 g of NaBH, over five minutes. Remove the cold-water bath and allow the reaction flask...
can someone please answer number one? im so lost DYES AND DYEING CHAPTER 1. Calculate the amounts of salicylic acid, 1-naphthol, 2-naphthol, 8-anilino-1-naph- thalenesulfonic acid ammonium salt, or N,N-dimethylaniline needed for Part 1B of this experiment (use molecules as assigned by your TA). 190mg 3-aminobenzene 2.5mL Sulfonic acid 2.5% sodium carbonate solution 81mg Sodium nitrate 2. What is the purpose of the sodium carbonate in Part 1A? Why do we add glacial acetic acid in Part 13 when we react...
Calculate the theoretical yield for Orange II (mw= 422g/mol; experimental weight of orange II azo-dye=0.4g). EXPERIMENTAL Calculate the theoretical yield before the lab. Caution: Orange II dyes clothing and other organic materials a permanent unique orange. As a measure of your technique, points may be subtracted for orange hands, etc. 1 DIAZOTIZATION OF SULFANILIC ACID Dissolve 0.4 g of anhydrous sodium carbonate in 7.5 mL of H.O. Use a 25 mL Erlenmever flask. 2. Add 0.45 g of sulfanilic acid...
this is the procedure of melting point experiment ( preparation acetanilid) I want the summarize of this procedure EXPERIMENTAL PROCEDURE Measure 0.100 to 0.125 g of aniline (in dropper bottles near the balances) into a tared reaction tube from the microscale kit and record the weight to the nearest milligram. Add 2 mL of distilled water and 6 to 7 drops (an excess amount, 21 drops =1 mL) of acetic anhydride. Stir the mixture for about 4 minutes untiha solid...
In this Diels-Alder reaction, what is the limiting reagent for this reaction? Please show work In this experiment, a Diels-Alder reaction will be performed to generate 4-cyclohexene- 1,2-dicarboxylic anhydride. The reaction occurs when 1,3-butadiene is combined with maleic anhydride and heated as shown below. Once the product has been isolated, the IR spectrum, melting point, and experimental yield can be determined. 5.- I111NI O Due to the inherent difficulties with the handling of gaseous 1,3-butadiene, it will be generated in...
Determine the theoretical yield and limiting reagent Running the Reaction Add 0.100 g benzil and 0.30 mL 95% ethanol to a 3-mL conical vial. Place a spin vane in the vial and attach an air condenser. Heat the mixture with an aluminum block (90-100°C) while stirring until the benzil has dissolved (see inset in Tech- nique 6, Figure 6.1A). Using a 9-inch Pasteur pipette, add dropwise 0.25 mL of an aqueous potassium hydroxide solution' downward through the condenser into the...
i need to calculate the theortetical yield by finding the limiting reactant of the experiment by converting reactants to product, then calculate the percent yield using the limiting reactant -in my experiment the amout of crystals i obtained was 1.232 g (watch glass + filter paper = 31.228 g and watch glass, filter paper, + crystals = 32.460 g) REACTION SCHEME H сно, ОН- ОСH, CH panisaldehyde acetophenone Molar Mass: 120.15g/mol Molar Mass: 136.15g/mol Molar Mass: 239.30g/mol Density: 1.119g/mL Density:...
Bromination of Acetanilide In a 25-mL Erlenmeyer flask, dissolve 0.68 g of acetanilide in approximately 4 mL glacial acetic acid. Record the exact amount of the limiting reactant that you used. Add a stir bar followed by 1.6 g pyridinium tribromide. Heat the mixture to ~60°C in a warm water bath for 10 minutes. After the 10 minutes, add 15 mL water and approximately 2 mL saturated sodium bisulfite solution to remove excess bromine, which shows by the disappearance of...