Draw a mechanism for a green aldol synthesis without solvent. using 3,4-dimethoxybenzaldehyde, 1-indanone, NaOH, HCl, ethanol and water
Above is the mechanism of aldol synthesis since the product is an aldol.
There is a probability of elimination of water molecule through acid catalysis as here HCl is used. Then the product will be aldol condensation product. The mechanism is given below-
Draw a mechanism for a green aldol synthesis without solvent. using 3,4-dimethoxybenzaldehyde, 1-indanone, NaOH, HCl, ethanol...
What is the expected mass of the product of the reaction of 0.0015 moles of 3,4-dimethoxybenzaldehyde and 0.0015 moles of 1-indanone with 0.05g of solid NaOH and addition of HCl solution afterwards? This is an aldol condensation (green chemistry) problem.
Provide a stepwise mechanism for the formation of 2-[(3,4-dimethoxyphenyl)methylene]-2,3-dihydro-1H-inden-1-one from 3,4-dimethoxybenzaldehyde and 1-indanone. Please show all steps! This is a crossed aldol condensation. Thanks! Crossed aldol condensation of 3,4-dimethoxybenzaldehyde and l-indanone CHO CH,0 NaOH spolu co m ments CH,O CH,09 enolate formation OH -H,0 T dehydration CHO OH O CH,0 CHOA carbonyl addition CH,0 initial aldol product
the top half of the image depicts the synthesis of 2-[(3,4-dimethoxyphenyl)methylene]-2,3-dihydro-1H-inden-1-one from 1-indanone and 3,4-dimethoxybenzaldehyde. The bottom half of the image attached shows the table of chemicals used in the reaction. How would I calculate theoretical yield and furthermore, the percent yield? This experiment had a lot of chemicals used and I don't know where to start. Crossed aldol condensation of 3.4-dimethoxybenzaldehyde and l-indanone your co m ments cholateOH -4.0 dehydration formation OH O CHOY carbonyl addition initial aldol product...
a) Draw mechanism/product for aldol reaction: NaOet ethanol (solvent) c) Final product if result is protonated with mild acid in an ice bath. d) Final product(s) it result is Awarmed) with excess H₃O+
Lab : Aldol Condensation Purpose. In this lab you will conduct the Aldol condensation reaction under solid-state reaction conditions that will involve grinding reactants in the solid phase. You must read ahead and learn about this reaction and the chemical mechanism for the Aldol condensation. There are two possible products which are the initial Aldol or subsequent elimination product. You will need to isolate and purify your reaction product. You will use your melting point, IR, 1H and 13C NMR spectra to...
Why is the benzaldehyde preferentially attacked by the 1-indanone over another 1-indanone? Using a mortar and pestle, grind approximately 5 g of sodium hydroxide into fine particles. Add 0.50 g of 3,4-dimethoxybenzaldehyde and 0.40 g of 1-indanone to a test tube. Using a vortex mixer, gently mix the two solids together, forming an oil. Add 0.10 g of finely ground sodium hydroxide from Step 1 to the oil. Allow the reaction to sit for 15 minutes. Add 4 mL of...
Aldol Condensation: 1) What is the purpose of using NaOH solution in this Aldol condensation? 2) Why acetic acid is used to wash the solid on the fiter? 3) Draw the structure of the product from the reaction: NaOH H +Acetone in ethanol
10.(7pts) Draw the mechanism for the following self Aldol Condensation. NaOH,H,O, heat Bonus: 5 pts no partial credit. All correct or nothing. Predict the product and draw a mechanism for the following transformation. Sune NaOET EtOH(solvent)
Draw the mechanism for the acid-chloride synthesis of ethyl butyrate using butyryl chloride, ethanol, sodium bicarbonate, and pyridine.
1. Provide the products for the following reactions (1 points). NaOH, Ethanol 2. Draw the mechanism for the reaction above (2 points). 3. Draw the 1H-NMR for the structure below. Label each peak on the NMR (2 points): DE H CE