If you used a reaction tube that is not completely dry in this Grignard Reaction experiment, what organic byproduct would you expect? How much water (in µL) would it take to react completely with the desired product? Show your calculation. (Presume that one H2O is needed for each RMgX.)
If you used a reaction tube that is not completely dry in this Grignard Reaction experiment,...
i need help with the prelab questions please Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
This is for the Grignard Reaction laboratory. Please help me answer this question, much appreciated. 1. If a student performing Laboratory with Grignard reaction accidently used acetone as the reaction solvent instead of diethyl ether, what would the major organic product(s) be? Draw the structure of the product(s) (no mechanism necessary). b. What was the purpose of adding magnesium sulfate in this experiment? c. Grignard reagents react with both aldehyde and ketone functional groups. How do you predict the reaction...
i need help with the postlab questions please Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
Grignard Reaction 1. Draw your complete reaction, including the formation of the Grignard reagent and the reaction with your carbonyl compound. Below each reagent, write its molecular weight and density (if a liquid). Also write how much of each material you will use in ml (if liquid), grams, and moles. Also include the molecular weight and melting point of your final product. 2. How many moles of Grignard reagent are you synthesizing? What mass of water could fully react with...
In Grignard reaction, the ether solvent must be very dry. What organic product is formed when phenyl magnesium bromide reacts with water? OH a b d OOOO
EXPERIMENT S: THE GRIGNARD REACTION Pre-lab assignments are found at the end of the lab manual Review the sections in Chapter 10 in the textbook dealing with organometalic reagents. As will be evident in this and chapters, Grignard reagents play a commanding role in organic synthesis, adaptable to the preparation of a large ater variety of functional systems, and comprise one of the major uses of alkyl halides. This experiment involves a synthesis diphenylmethanol using phenylmagnesium bromide and benzaldehyde Reaction...
In an experiment we used, Grignard reagent reacted with benzophenone, in a two stepped process in order to create triphenylmethanol If you use excess Grignard reagent in this reaction, what contaminant would it yield after hydrolysis with HCl? Would you expect this contaminant to be removed in the extraction step?
Experiment 2: Grignard synthesis of benzoic acid . Complete reaction, and provide the reaction mechanism for all chemistry in this lab (forming the Grignard reagent, reaction with the CO2 electrophile, and acidification). . What are the side products and salts formed in this reaction? How are they removed from the purified product? . Why do we take precautions to eliminate water from the reaction? Be specific about what would happen if we did not do so. . Why is the...
Grignard Reaction with a Ketone: Triphenylmethanol Introduction: The purpose of this lab is to prepare phenylmagnesium bromide, a Grignard reagent, and react it with benzophenone to give triphenylmethanol. Grignard reagents are very reactive and must be synthesized in an environment free of water or any other source of potential proton donor. Once made, the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone, benzophenone. The result is an alkoxide that is then protonated to give...
We preformed an Grignard Reaction in Organic Chemistry lab. Benzophenone + Phenylmagnesium Chloride (2M in THF) + Diethyl Ether -> triphenylmethanol This may help: Below are IRs of Benzophenone and Trimethylmethanol. We performed a Grignard reaction to get an alcohol product from a ketone. I am having trouble with the peaks. They do not look great and the sample IR on the Benzophenone's Ketone peak is not where I would expect. Please help me characterize this. Note: We were unable...